Purification of Laboratory Chemicals

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Purification of Laboratory Chemicals

ISBN: 0750675713
Title: Purification of Laboratory Chemicals
Author: W L F Armarego
Publisher: Butterworth-Heinemann

Summary:
Now in its fifth edition, the book has been updated to include more detailed descriptions of new or more commonly used techniques since the last edition as well as remove those that are no longer used, procedures which have been developed recently, ionization constants (pKa values) and also more detail about the trivial names of compounds.

In addition to having two general chapters on purification procedures, this book provides details of the physical properties and purification procedures, taken from literature, of a very extensive number of organic, inorganic and biochemical compounds which are commercially available. This is the only complete source that covers the purification of laboratory chemicals that are commercially available in this manner and format.

* Complete update of this valuable, well-known reference
* Provides purification procedures of commercially available chemicals and biochemicals
* Includes an extremely useful compilation of ionisation constants
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Table of Contents
Preface to the Fifth Edition
Preface to the First Edition
Preface to the Second Edition
Preface to the Third Edition
Preface to the Fourth Edition
Common Physical Techniques Used in Purification p. 1
Introduction p. 1
The Question of Purity p. 1
Safety Precautions Associated with the Purification of Laboratory Chemicals p. 4
Methods of Purification of Reagents and Solvents p. 6
Distillation p. 8
Recrystallisation p. 14
Sublimation p. 17
Chromatography p. 17
Abbreviations p. 30
Tables p. 30
Bibliography p. 45
Chemical Methods Used in Purification p. 53
General Remarks p. 53
Removal of Traces of Metals from Reagents p. 53
Use of Metal Hydrides p. 55
Purification via Derivatives p. 56
General Methods for the Purification of Classes of Compounds p. 60
General Procedures for the Purification of Some Classes of Organic Compounds p. 61
Bibliography p. 70
The Future of Purification p. 72
Introduction p. 72
Solid Phase Synthesis p. 72
Ionic Liquids p. 77
Fluorous Chemistry p. 77
Bibliography p. 78
Purification of Organic Chemicals p. 80
Purification of Inorganic and Metalorganic Chemicals (Including Organic compounds of B, Bi, P, Se, Si, and ammonium and metal salts of organic acids) p. 389
Purification of Biochemicals and Related Products p. 500
General Subject Index p. 578
CAS Registry Numbers Index p. 585

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